Hello,
While a pot furnace will give you a good thermal soak, I wonder just how much accurate control you have over the annealing process itself. Keep in mind that the prior thermal and mechanical history needs to be known as recrystallization and annealing occur much faster in a more heavily cold worked alloy. Excessive grain growth can result from too much time at temperature. Possibly there is no recirculating air in your pot furnace and thus thermal stratification can occur.
You can purchase the following books and specifications or perhaps there is a technical or a local engineering library with these already in it.
(1) ASTM B601 gives multiple sets of annealing tempers for copper & its alloys, some based upon prior mechanical processing, some based upon grain size.
For example:
- OS005 is annealed, with final average grain size of 0.005 mm.
- OS200 is annealed, with final average grain size of 0.200 mm.
- O81 is an 'Annealed to' temper - Hard material annealed down to 1/4 Hard.
(1a) ASTM B601-07 Standard Classification for Temper Designations for Copper and Copper Alloys—Wrought and Cast.
www.astm.org/cgi-bin/SoftCart.exe/DATABA...m?L+mystore+eulz4392
(2)Books from The American Society for Metals (ASM)
(a) - Handbook Volume 2 Nonferrous Metals
(b) - Handbook Volume 4 Heat Treating
(c) - Heat Treater's Guide: Practices and Procedures for Nonferrous Alloys.
See:
www.asminternational.org/Content/Navigat...ks/ASM_Handbooks.htm
Book (c) may be the one most important for you. The non-member price is $US 251.00.
Finally, I reviewed EBNER Industrieofenbau Gesellschaft m.b.H., a well renowned manufacturer of copper and copper alloy batch annealers in Austria, (
www.ebnerhicon.at/ ) and I saw no pot furnaces for copper alloys.
Perhaps, as you have already suspected, this is your basic problem. Some experimentation with a small but accurate annealer at some other location will provide you with the answers you are looking for.
Kindest regards,
Peter J. Stewart-Hay
Principal
Stewart-Hay Associates
www.Stewart-Hay.com